HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glyceraldehyde → 4-(n-Hexadecylamino)benzoyl glyceraldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glyceraldehyde | HCID 751 | — |
| Edukt | Chloroform | HCID 6212 | — |
| Edukt | 4-Hexadecylaminobenzoyl chloride hydrochloride | HCID 13255322 | — |
| Katalysator | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 4-(n-Hexadecylamino)benzoyl glyceraldehyde | HCID 21326953 | — |
Reaktionsschritte
To a mixture of 3.6 g. of glyceraldehyde and 2.44 g. of 4-dimethylaminopyridine in an ice-bath is added 4.16 g. of 4-(n-hexadecylamino)benzoyl chloride hydrochloride. After 4 hours at room temperature, chloroform and water are added. The chloroform extract is chromatographed quickly and evaporated in vacuo to yield 4-(n-hexadecylamino)benzoyl glyceraldehyde.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04146546 |
| Quelldatensatz | uspto-grants-1979_03 |
| ORD ID | ord-66fef1a1db6948c9940bcde96e59a27b |
| Quellennotiz | uspto-grants-1979_03 |