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HRID 615095Erstellt: 25. Oktober 2026

Acetone → 7,8-Dichloro-1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one

https://huagongshe.com/reaction/615095

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetoneHCID 180—
EduktMethyl IsocyanateHCID 12228—
Edukt2-Amino-5,6-dichlorobenzimidazoleHCID 466016—
Produkt7,8-Dichloro-1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-oneHCID 135797529—

Reaktionsschritte

Reaction of 2-amino-5,6-dichlorobenzimidazole with acetone and methyl isocyanate according to the procedure of Example 1, first paragraph, provided the title compound. In this case, a 10-N-methylcarbamoyl derivative was not isolated from the reaction mixture. The product was recrystallized from acetone to give a solid, mp 220° C. (dec.). The confirmatory elemental analysis is shown in Table III.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04497650
Quelldatensatzuspto-grants-1985_02
ORD IDord-26ae51d292ef4f89b80d7fdd7ac69716
Quellennotizuspto-grants-1985_02