HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetone → 7,8-Dichloro-1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetone | HCID 180 | — |
| Edukt | Methyl Isocyanate | HCID 12228 | — |
| Edukt | 2-Amino-5,6-dichlorobenzimidazole | HCID 466016 | — |
| Produkt | 7,8-Dichloro-1,2-dihydro-2,2,3-trimethyl-1,3,5-triazino[1,2-a]benzimidazol-4(3H)-one | HCID 135797529 | — |
Reaktionsschritte
Reaction of 2-amino-5,6-dichlorobenzimidazole with acetone and methyl isocyanate according to the procedure of Example 1, first paragraph, provided the title compound. In this case, a 10-N-methylcarbamoyl derivative was not isolated from the reaction mixture. The product was recrystallized from acetone to give a solid, mp 220° C. (dec.). The confirmatory elemental analysis is shown in Table III.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04498920 |
| Quelldatensatz | uspto-grants-1985_02 |
| ORD ID | ord-99e8f81173784a4e8d0d12ff3f86fd1d |
| Quellennotiz | uspto-grants-1985_02 |