Hydrochloric Acid → HCID 70477797, Verbindung

HRID 615308

Reaktionsgleichung

Reaktionsgleichung von HRID 615308
[Cl-].[Al+3].[Cl-].[Cl-].[C:5](Cl)(=[O:7])[CH3:6].C(Cl)(Cl)(Cl)Cl.[Al+3].[Cl-].[Cl-].[Cl-].[C:18]1([CH:24]([CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH3:43])[C:25]([OH:27])=[O:26])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.Cl>C(Cl)(Cl)(Cl)Cl>[C:5]([C:24]([C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)([CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH3:43])[C:25]([OH:27])=[O:26])(=[O:7])[CH3:6]

Komponenten

7

Edukt 5

HCID 313Hydrochloric AcidHCID 6367Acetyl chlorideHCID 6451240Aluminum(III) ChlorideHCID 220152372-Phenyloctadecanoic acidHCID 131714100HCID 131714100, Verbindung

Produkt 1

HCID 70477797HCID 70477797, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 5943Carbon TetrachlorideLösungsmittel3×

Versuchsvorschrift

A 500 ml reaction vessel was charged with 200 mls freshly distilled carbon tetrachloride and the CCl4 was cooled to 0°-5° C. Aluminum chloride (0.33 moles) was added, via Gooch tubing, to the CCl4 over a period of 20 minutes. Acetyl chloride (0.35 mol) was added to an addition funnel and charged to the CCl4 -AlCl3 mixture. Phenylstearic acid (0.125 moles) was then slowly added to the reaction mixture from an addition funnel while maintaining the temperature of the reaction mixture at 0°-5° C. The temperature was maintained at 0°-5° C. for one hour and at room temperature for an additional two hours. The evolution of HCl was observed.

Aufarbeitung

  1. customA 500 ml reaction vessel
  2. temperaturewhile maintaining the temperature of the reaction mixture at 0°-5° C

Quellen und Nachweise

ORD-Eintrag
ord-81c1187f66ae4a17949542ab91d3be67
Quelldatensatz
uspto-grants-1985_02
Patentnummer
US04499013

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