HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diisopropylamine → HCID 13272378, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diisopropylamine | HCID 7912 | — |
| Edukt | Ethyl chloroformate | HCID 10928 | — |
| Edukt | 3-Isoquinolinecarboxylicacid, 1-(2-chlorophenyl)- | HCID 11000554 | — |
| Lösungsmittel | Triethylamine | HCID 8471 | — |
| Produkt | HCID 13272378 | HCID 13272378 | 23,2% |
Reaktionsschritte
Operations are carried out as for Example 7, starting from 2.83 g of 1-(2-chloro phenyl) isoquinoline 3-carboxylic acid, 1.17 g of triethylamine, 1.25 g of ethyl chloroformate and 1.31 g of di-isopropylamine in 100 ml of chlorofom. 0.85 g of N,N-di(1-methyl ethyl) 1-(2-chloro phenyl) isoquinoline 3-carboxamide, melting at 161° C., is obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04499094 |
| Quelldatensatz | uspto-grants-1985_02 |
| ORD ID | ord-782300f7520f40ef882ecfdb198c7fef |
| Quellennotiz | uspto-grants-1985_02 |