HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclooctylamine → 7-(2-Hydroxy-3-cyclooctylaminopropoxy)-isoflavone hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclooctylamine | HCID 2903 | — |
| Edukt | 7-(2,3-Epoxypropoxy)-3-phenylchromone | HCID 10108482 | — |
| Edukt | Ethanol hydrochloride | HCID 21887872 | — |
| Lösungsmittel | Isopropanol | HCID 3776 | — |
| Produkt | 7-(2-Hydroxy-3-cyclooctylaminopropoxy)-isoflavone hydrochloride | HCID 20406830 | — |
Reaktionsschritte
Using Method B, the reaction of 7-(2,3-epoxypropoxy)isoflavone with cyclooctylamine followed by acidification of the resulted free base with HCl/EtOH gave the hydrochloride as light yellow prisms, m.p. 185°-186° (iPrOH).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04501755 |
| Quelldatensatz | uspto-grants-1985_02 |
| ORD ID | ord-774675ad157e41fdb4a0d7016dfe625b |
| Quellennotiz | uspto-grants-1985_02 |