HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl iodide → 2,3-Pentanedione, 2-(O-methyloxime)
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 2,3-Pentanedione, 2-oxime | HCID 6797453 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 2,3-Pentanedione, 2-(O-methyloxime) | HCID 54196011 | — |
Reaktionsschritte
49.7 g (0.35 mol) of methyl iodide are added dropwise at room temperature to a solution of 40.2 g (0.55 mol) of pentane-2,3-dione 2-oxime and 52.0 g (0.38 mol) of potassium carbonate in 400 ml of acetone, and stirring is continued for 12 hours at this temperature.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05948932 |
| Quelldatensatz | uspto-grants-1999_09 |
| ORD ID | ord-56b9c51c8bf34f14bc300d585182814c |
| Quellennotiz | uspto-grants-1999_09 |