Hydrochloric Acid → Ethyl 3-methylbenzimidate hydrochloride
Reaktionsgleichung
[C:1]1([CH3:9])[CH:6]=[CH:5][CH:4]=[C:3]([C:7]#[N:8])[CH:2]=1.[ClH:10].[CH2:11]([OH:13])[CH3:12]>>[ClH:10].[CH3:9][C:1]1[CH:2]=[C:3]([CH:4]=[CH:5][CH:6]=1)[C:7](=[NH:8])[O:13][CH2:11][CH3:12]Komponenten
4
Versuchsvorschrift
Ethyl 3-methylbenzimidate hydrochloride was synthesized in the same manner as in Reference Example 2. That is, m-tolunitrile (25.2 g, 0.215 mol) was treated with hydrogen chloride in ethanol (250 mL) to give 41.7 g (97%) of the target compound as colorless crystals.
Quellen und Nachweise
- ORD-Eintrag
- ord-472e9956c224470ca9bd5bd552bcd52d
- Quelldatensatz
- uspto-grants-1999_09
- Patentnummer
- US05948785
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