Hydrochloric Acid → HCID 12282158, Verbindung
Reaktionsgleichung
[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][CH:3]=1.Cl.[CH2:11]([OH:13])[CH3:12]>>[ClH:1].[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([C:6](=[NH:7])[O:13][CH2:11][CH3:12])=[CH:4][CH:3]=1Komponenten
4
Versuchsvorschrift
Ethyl 4-chlorobenzimidate hydrochloride was synthesized in the same manner as in Reference Example 2. That is, p-chlorobenzonitrile (25.6 g, 0.186 mol) was reacted with hydrogen chloride in ethanol (250 mL) to give 36.8 g (90%) of the target compound as colorless crystals.
Quellen und Nachweise
- ORD-Eintrag
- ord-0c88e10afcb24685bc08ebf483a811ea
- Quelldatensatz
- uspto-grants-1999_09
- Patentnummer
- US05948785
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