HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phthalic Anhydride → 2-(6-hydroxyhexyl)-2,3-dihydro-1H-isoindole-1,3-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phthalic Anhydride | HCID 6811 | — |
| Edukt | 6-Amino-1-hexanol | HCID 19960 | — |
| Edukt | 5-Phthalimidohexanol | HCID 12781348 | — |
| Produkt | 2-(6-hydroxyhexyl)-2,3-dihydro-1H-isoindole-1,3-dione | HCID 12950219 | 91% |
Reaktionsschritte
This compound was prepared in the same manner as 5-phthalimidohexanol from 6-aminohexanol (3.51 g, 30.0 mmol) and phthalic anhydride (4.44 g, 30.0 mmol) to give the product as brown oil: yield 91%; 1H NMR (CDCl3) δ 1.3-1.8 (m, 8H), 3.6-3.7 (m, 4H), 4.3 (t, J=6.5 Hz, 1H), 7.7 (m, 2H), 7.8 (m, 2H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05952307 |
| Quelldatensatz | uspto-grants-1999_09 |
| ORD ID | ord-94ff5347b5c24f60b32c4bbfe3402c6a |
| Quellennotiz | uspto-grants-1999_09 |