HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Iodohexane → Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hexyloxy-2-naphthyl]benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Iodohexane | HCID 12527 | — |
| Edukt | Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000320 | — |
| Produkt | Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hexyloxy-2-naphthyl]benzoate | HCID 22000297 | 55% |
Reaktionsschritte
Following the procedure of Example 1(a), but reacting 430 mg (1 mmol) of methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 180 μl (1.2 mmol) of 6-iodohexane, 280 mg (55%) of methyl 2-hydroxy-4-[7-(1-adamantyl)-6-hexyloxy-2-naphthyl]benzoate were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05952382 |
| Quelldatensatz | uspto-grants-1999_09 |
| ORD ID | ord-4c1e3c9840214f13b9f2df01de932ffa |
| Quellennotiz | uspto-grants-1999_09 |