HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 4-iodobenzoate → Methyl 4-[7-(1-adamantyl)-6-benzyloxy-2-naphthyl]benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 4-iodobenzoate | HCID 69273 | — |
| Edukt | 7-(1-Adamantyl)-6-benzyloxy-2-naphthylboronic acid | HCID 22000313 | — |
| Produkt | Methyl 4-[7-(1-adamantyl)-6-benzyloxy-2-naphthyl]benzoate | HCID 22000300 | 33,5% |
Reaktionsschritte
Following the procedure of Example 1(c), but reacting 1.5 g (3.6 mmol) of 7-(1-adamantyl)-6-benzyloxy-2-naphthylboronic acid with 500 mg (1.9 mmol) of methyl 4-iodobenzoate, 320 mg (33%) of the compound were obtained, which compound had a melting point of 170°-3° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05952382 |
| Quelldatensatz | uspto-grants-1999_09 |
| ORD ID | ord-44fbc64ee8794188a119649a305c5468 |
| Quellennotiz | uspto-grants-1999_09 |