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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 61970Erstellt: 27. Oktober 2026

Salicylic Acid → HCID 178455906, Verbindung

https://huagongshe.com/reaction/61970

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktSalicylic AcidHCID 338—
EduktCID 86674079HCID 86674079—
LösungsmittelAcetonitrile--water (1/1)HCID 18373917—
ProduktHCID 178455906HCID 178455906—

Reaktionsschritte

Salicylic acid (138.12 g/mol, 0.15 mg) 1.5 mg salicylic acid was dissolved in 100 μl ACN/H2O 50/50 mixture to give the mother solution. 10 μl of this latter solution were then added to 0.76 mg exendin-4 acetate dissolved in 50 μl ACN/H2O 50/50 followed by speedvac 2×1 hour as above at approximately 35° C., affording exendin-4 salicylate as a white solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09445992B2
Quelldatensatzuspto-grants-2016_09
ORD IDord-a82eea5de7aa439dba4c27bf304e8613
Quellennotizuspto-grants-2016_09