HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Chloro-4-nitrobenzene → 1,3-Bis(4-nitrophenoxy)-2,2,4-trimethylpentane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Chloro-4-nitrobenzene | HCID 7474 | — |
| Edukt | 2,2,4-Trimethyl-1,3-pentanediol | HCID 8946 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Lösungsmittel | Dimethyl Sulfoxide | HCID 679 | — |
| Produkt | 1,3-Bis(4-nitrophenoxy)-2,2,4-trimethylpentane | HCID 19860678 | — |
Reaktionsschritte
146 g (1 mol) 2,2,4-trimethyl-1,3-dihydroxypentane, 346.5 g (2.2 mols) 4-nitrochlorobenzene and 140 g powdered sodium hydroxide were reacted using the same procedure described in Example 1 in 600 ml DMSO.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04820866 |
| Quelldatensatz | uspto-grants-1989_04 |
| ORD ID | ord-81048ea7faf3483092d2da47a242376d |
| Quellennotiz | uspto-grants-1989_04 |