HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N,N-Dimethylmethanesulphonamide → HCID 21291506, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N,N-Dimethylmethanesulphonamide | HCID 70191 | — |
| Edukt | Ethyl 2-amino-5-methoxybenzoate | HCID 21291483 | — |
| Edukt | Butyllithium | HCID 178418339 | — |
| Produkt | HCID 21291506 | HCID 21291506 | — |
Reaktionsschritte
In a similar manner to that described in Example 12(a), N,N-dimethylmethanesulphonamide was reacted with n-butyl lithium and the product was reacted with ethyl 2-amino-5-methoxybenzoate to give the novel compound 1-(2-amino-5-methoxyphenyl)-2-(N,N-dimethylsulphamoyl)ethanone, m.p. 198°-200°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04772614 |
| Quelldatensatz | uspto-grants-1988_09 |
| ORD ID | ord-87820ce0e9544d7c91daa3f8a707e23e |
| Quellennotiz | uspto-grants-1988_09 |