Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | p-Toluenesulfonic acid | HCID 6101 | — |
| Edukt | Galactaric acid | HCID 3037582 | — |
| Katalysator | HCID 178477782 | HCID 178477782 | — |
| Lösungsmittel | Heptanol | HCID 8129 | — |
| Produkt | Diheptyl galactarate | HCID 131737197 | — |
Reaktionsschritte
In one specific embodiment of the present disclosure, 20 ml of 1-heptanol, 1 mmol of galactaric acid, 0.05 mmol of methyltrioxorhenium catalyst, and 0.05 mmol of para-toluenesulfonic acid were poured into a 50 cc reactor. The temperature in the reactor was then raised to 150° C. and the reaction was performed for 12 hours, maintaining the reactor temperature at 150° C. to obtain diheptyl galactarate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US09447012B2 |
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| Quelldatensatz | uspto-grants-2016_09 |
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| ORD ID | ord-f5e7bc175fbd42759b8032b4cebdc309 |
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| Quellennotiz | uspto-grants-2016_09 |
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