2-Acetoxybenzoyl chloride → 3-Acetamidobicyclo[1.1.1]pentan-1-yl 2-acetoxybenzoate

HRID 62621

Reaktionsgleichung

Reaktionsgleichung von HRID 62621
[OH:1][C:2]12[CH2:6][C:4]([NH:7][C:8](=[O:10])[CH3:9])([CH2:5]1)[CH2:3]2.[CH3:11][C:12]([O:14][C:15]1[C:20]([C:21](Cl)=[O:22])=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:13]>>[C:12]([O:14][C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][C:20]=1[C:21]([O:1][C:2]12[CH2:6][C:4]([NH:7][C:8](=[O:10])[CH3:9])([CH2:5]1)[CH2:3]2)=[O:22])(=[O:13])[CH3:11]

Komponenten

3

Edukt 2

HCID 796682-Acetoxybenzoyl chlorideHCID 86287953N-{3-hydroxybicyclo[1.1.1]pentan-1-yl}acetamide

Produkt 1

HCID 862880273-Acetamidobicyclo[1.1.1]pentan-1-yl 2-acetoxybenzoate

Versuchsvorschrift

The general procedure of Example 1 Step 3 is repeated starting with N-(3-hydroxybicyclo[1.1.1]pentan-1-yl)acetamide (1) and using O-acetylsalicyloyl chloride in place of the acetyl chloride to produce compound 8.

Quellen und Nachweise

ORD-Eintrag
ord-89ab6e73474a4b8c9d4257835a570368
Quelldatensatz
uspto-grants-2016_09
Patentnummer
US09447026B2

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