HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → HCID 58107439, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 3-(Chlorosulfonyl)-4-fluorobenzoic acid | HCID 3929891 | — |
| Katalysator | Dimethylformamide | HCID 6228 | — |
| Produkt | HCID 58107439 | HCID 58107439 | — |
Reaktionsschritte
3-(Chlorosulfonyl)-4-fluorobenzoic acid (1, 2.50 g, 10.5 mmol), thionyl chloride (10 mL) and DMF (1 drop) were heated at 90° C. for 1 hour and then the mixture evaporated to dryness. The material was used directly in the next step.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09309283B2 |
| Quelldatensatz | uspto-grants-2016_04 |
| ORD ID | ord-0d81ebdcd29843118ce9e289125ed5c6 |
| Quellennotiz | uspto-grants-2016_04 |