HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Ethylpyridin-2-amine → 4-Ethyl-5-iodopyridin-2-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Ethylpyridin-2-amine | HCID 118425 | — |
| Edukt | N-Iodosuccinimide | HCID 120273 | — |
| Produkt | 4-Ethyl-5-iodopyridin-2-amine | HCID 58200578 | — |
Reaktionsschritte
The title compound is synthesized according to general procedure GP1 starting from 5.0 g (41 mmol) 4-ethyl-pyridin-2-ylamine and 9.2 g (41 mmol) NIS. Yield after precipitation from the reaction mixture and isolation of additional product from the mother liquid by chromatography using silica gel: 10.3 g (100%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09321771B2 |
| Quelldatensatz | uspto-grants-2016_04 |
| ORD ID | ord-31ac751b417241f29671fdeaa6defe72 |
| Quellennotiz | uspto-grants-2016_04 |