HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Homophenylalanine, DL- → 2-Amino-4-phenylbutan-1-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Homophenylalanine, DL- | HCID 102530 | — |
| Edukt | Aluminium lithium hydride | HCID 21226445 | — |
| Produkt | 2-Amino-4-phenylbutan-1-ol | HCID 13145036 | 78,1% |
Reaktionsschritte
Following the general procedure of example 40b, DL-homophenylalanine (5.0 g, 27.9 mmol) was reduced with LiAlH4 to give (RS)-2-amino-4-phenyl-butan-1-ol (3.6 g, 78%, MS: m/e=166 (M+H+)) as a light yellow solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06184236B2 |
| Quelldatensatz | uspto-grants-2001_02 |
| ORD ID | ord-922d82ec72894955b59b642a49546f4e |
| Quellennotiz | uspto-grants-2001_02 |