Diethyl ethylmalonate → 2-Amino-2-ethyl-4-[4-(1-hydroxyoctyl)phenyl]butanol

HRID 635479Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 635479
C([O:4][CH2:5][C:6]([NH:26]C(=O)C)([CH2:24][CH3:25])[CH2:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]([C:15](=[O:23])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[CH:11][CH:10]=1)(=O)C.C(OC(=O)C(CC)C(OCC)=O)C>>[NH2:26][C:6]([CH2:24][CH3:25])([CH2:7][CH2:8][C:9]1[CH:10]=[CH:11][C:12]([CH:15]([OH:23])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[CH:13][CH:14]=1)[CH2:5][OH:4]

Komponenten

3

Edukt 2

HCID 8610Diethyl ethylmalonateHCID 53718772HCID 53718772, Verbindung

Produkt 1

HCID 226187962-Amino-2-ethyl-4-[4-(1-hydroxyoctyl)phenyl]butanol

Versuchsvorschrift

In working example 77, 2-acetamido-2-ethyl-4-(4-octanoylphenyl)butyl acetate obtained by using ethylmalonic acid diethyl ester instead of propylmalonic acid diethyl ester, is treated in the same manners as working example 79 and then working example 80 to give the subject compound.

Aufarbeitung

  1. customobtained
  2. additionis treated in the same manners
  3. customto give the subject compound

Quellen und Nachweise

ORD-Eintrag
ord-df0000f5f6fc4f178a75fe6914b3b386
Quelldatensatz
uspto-grants-2001_02
Patentnummer
US06187821B1

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