HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 636336Erstellt: 26. Oktober 2026
Dinitrofluorobenzene → N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine
https://huagongshe.com/reaction/636336
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Dinitrofluorobenzene | HCID 6264 | — |
| Edukt | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Edukt | 3-(Heptadecafluorooctyl)aniline | HCID 4245356 | — |
| Lösungsmittel | Triethylamine | HCID 8471 | — |
| Produkt | N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine | HCID 22735001 | 83,2% |
Reaktionsschritte
A mixture of 3-(perfluoro-n-octyl)benzenamine (2.04 g), 2,4-dinitrofluorobenzene (0.78 g), NMP (8 mL) and triethylamine (0.85 mL) was heated to 70° C. for 16 hr. Extraction and recrystallization from hexane-ethyl acetate gave N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine (2.25 g, mp 124.5-125° C.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US06194039B1 |
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| Quelldatensatz | uspto-grants-2001_02 |
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| ORD ID | ord-675ff4d0296243a691641a083f5f49c7 |
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| Quellennotiz | uspto-grants-2001_02 |
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