1,6-Hexanediol → 1,6-Hexanediol adipoyl chloride
Reaktionsgleichung
[C:1]([Cl:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([Cl:8])=[O:7].C(O)CCCCCO>C(N(CC)CC)C>[CH2:1]([OH:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][OH:7].[C:1]([Cl:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([Cl:8])=[O:7]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Next, the adipoyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 3 minutes. Consequently, adipoyl chloride condensed on the surface of the base particles. A polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place between adipoyl chloride condensed on the surface of the base particles and 1,6-hexanediol contained therein, forming a film of 1,6-hexanediol-adipoyl chloride co-polymer on the surface of the base particles.