Ethylene Glycol → Ethylene glycol sebacoyl chloride

HRID 636794

Reaktionsgleichung

Reaktionsgleichung von HRID 636794
[C:1]([Cl:14])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([Cl:12])=[O:11].C(N(CC)CC)C.[CH2:22]([OH:25])[CH2:23][OH:24]>>[CH2:22]([OH:25])[CH2:23][OH:24].[C:10]([Cl:12])(=[O:11])[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][C:1]([Cl:14])=[O:13]

Komponenten

4

Edukt 3

HCID 174Ethylene GlycolHCID 8471TriethylamineHCID 66072Sebacoyl chloride3×

Produkt 1

HCID 86756477Ethylene glycol sebacoyl chloride

Versuchsvorschrift

The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of sebacoyl chloride in the mixing section 22. Next, in the mixing section 22, the vapor of sebacoyl chloride was cooled, and the introduced base particles were exposed thereto for 2 minutes. Consequently, a polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place on the surface of the base particles between sebacoyl chloride and ethylene glycol, forming a film of ethylene glycol-sebacoyl chloride co-polymer.

Aufarbeitung

  1. temperatureThe base particles, along with helium gas, were cooled
  2. customConsequently, a polymerization reaction

Quellen und Nachweise

ORD-Eintrag
ord-e6a203c38b194da688c631e0db90473d
Quelldatensatz
uspto-grants-2001_02
Patentnummer
US06194487B1

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