HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sulfuryl chloride → 2,3-dihydro-5H-benzo[f][1,4]oxazepine-4-sulfonyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sulfuryl chloride | HCID 24648 | — |
| Edukt | Diisopropylethylamine | HCID 81531 | — |
| Edukt | 2,3,4,5-Tetrahydro-1,4-benzoxazepine | HCID 21882775 | — |
| Edukt | 7-methoxy-3,4-dihydro-1H-isoquinoline-2-sulfonyl chloride | HCID 22665676 | — |
| Produkt | 2,3-dihydro-5H-benzo[f][1,4]oxazepine-4-sulfonyl chloride | HCID 22665777 | — |
Reaktionsschritte
This compound was prepared from 1.5 g of 2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine, 0.81 mL of sulfuryl chloride and 1.8 mL of ethyl diisopropyl amine using the procedure described for 63f. Yield: 0.3 g (oil), EI-MS: 247 (M+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06194409B1 |
| Quelldatensatz | uspto-grants-2001_02 |
| ORD ID | ord-451befc9eacd48408744e619c852f3af |
| Quellennotiz | uspto-grants-2001_02 |