HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 637256Erstellt: 25. Oktober 2026
3-(Chlorocarbonyl)phenyl acetate → N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine
https://huagongshe.com/reaction/637256
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 3-(Chlorocarbonyl)phenyl acetate | HCID 12998558 | — |
| Edukt | Dimethyl sulphoximine potassium salt | HCID 86740516 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine | HCID 20256530 | — |
Reaktionsschritte
A solution of 99.3 g of m-acetoxybenzoyl chloride in 150 ml of absolute tetrahydrofuran is added dropwise at -35° C. during 20 minutes while stirring to the dimethyl sulphoximine potassium salt suspension and the mixture is then stirred at -35° C. for 30 minutes. N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine is thus formed in suspension.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04556413 |
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| Quelldatensatz | uspto-grants-1985_12 |
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| ORD ID | ord-7abe3c7ad9e0455ab3840a266774c0b4 |
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| Quellennotiz | uspto-grants-1985_12 |
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