Methyl 3-(hex-3-en-1-yl)-4,5-dimethoxybenzoate → Methyl 3-hexyl-4,5-dimethoxybenzoate

HRID 638920Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 638920
[CH3:1][O:2][C:3](=[O:20])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([O:12][CH3:13])=[C:6]([CH2:14][CH2:15][CH:16]=[CH:17][CH2:18][CH3:19])[CH:5]=1>CCOC(C)=O>[CH3:1][O:2][C:3](=[O:20])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([O:12][CH3:13])=[C:6]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[CH:5]=1

Komponenten

3

Edukt 1

HCID 68684188Methyl 3-(hex-3-en-1-yl)-4,5-dimethoxybenzoate

Produkt 1

HCID 68685356Methyl 3-hexyl-4,5-dimethoxybenzoate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8857Ethyl AcetateLösungsmittel

Versuchsvorschrift

3-Hexyl-4,5-dimethoxybenzoic acid methyl ester was prepared from 3-hex-3-enyl-4,5-dimethoxybenzoic acid methyl ester by following Method H using EtOAc as a solvent. The reaction was conducted for 2.5 h under hydrogen atmosphere. The product obtained in quantitative yield was used without further purification.

Aufarbeitung

  1. customThe product obtained in quantitative yield
  2. customwas used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-d6e16dcf34144d11a431166a278f78a2
Quelldatensatz
uspto-grants-2010_04
Patentnummer
US07691843B2

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