Methylparaben → Methyl 4-((6-methylpyridin-2-yl)methoxy)benzoate
Reaktionsgleichung
[CH3:1][O:2][C:3](=[O:11])[C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][CH:5]=1.Cl.Cl[CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([CH3:21])[N:16]=1>>[CH3:1][O:2][C:3](=[O:11])[C:4]1[CH:9]=[CH:8][C:7]([O:10][CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([CH3:21])[N:16]=2)=[CH:6][CH:5]=1Komponenten
3
Versuchsvorschrift
The title compound is prepared in a manner substantially analogous to Procedure E except KI (1.3 eq.) is also added from 4-hydroxy-benzoic acid methyl ester and 2-(chloromethyl)-6-methyl-pyridine hydrochloride [CAS 3099-29-4]. MS (ES+) 258.2
Quellen und Nachweise
- ORD-Eintrag
- ord-b695783cef3a423b88f9137f84e17478
- Quelldatensatz
- uspto-grants-2010_04
- Patentnummer
- US07696234B2
Notizen zur Reaktion
Wird geladen…