HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl 5-chloroindole-2-carboxylate → 5-Chloro-1-naphthalen-1-ylmethyl-1H-indole-2-carboxylic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl 5-chloroindole-2-carboxylate | HCID 78518 | — |
| Edukt | 1-(Bromomethyl)naphthalene | HCID 137844 | — |
| Produkt | 5-Chloro-1-naphthalen-1-ylmethyl-1H-indole-2-carboxylic acid | HCID 58900241 | — |
Reaktionsschritte
Using general procedure B, 5-chloro-1H-indole-2-carboxylic acid ethyl ester was coupled with 1-bromomethyl-naphthalene and the product obtained was hydrolyzed to give the title compound as a white solid. MS: 334.0 ([M−H]−).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07696240B2 |
| Quelldatensatz | uspto-grants-2010_04 |
| ORD ID | ord-999fcc08a16147dd8c7a54fac6107e7c |
| Quellennotiz | uspto-grants-2010_04 |