1-(Bromomethyl)naphthalene → HCID 58900231, Verbindung
Reaktionsgleichung
C[O:2][C:3]([C:5]1[NH:6][C:7]2[C:12]([CH:13]=1)=[CH:11][CH:10]=[C:9]([CH3:14])[CH:8]=2)=[O:4].Br[CH2:16][C:17]1[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[CH:20]=[CH:19][CH:18]=1>>[CH3:14][C:9]1[CH:8]=[C:7]2[C:12]([CH:13]=[C:5]([C:3]([OH:2])=[O:4])[N:6]2[CH2:16][C:17]2[C:26]3[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=3)[CH:20]=[CH:19][CH:18]=2)=[CH:11][CH:10]=1Komponenten
3
Versuchsvorschrift
Using general procedure B, 6-methyl-1H-indole-2-carboxylic acid methyl ester was coupled with 1-bromomethyl-naphthalene and the product obtained was hydrolyzed to give the title compound as a white solid. MS: 314.1 ([M−H]−).
Aufarbeitung
- customthe product obtained
Quellen und Nachweise
- ORD-Eintrag
- ord-5e6c4962f7c94a6f8acfa2d0c2ab6b82
- Quelldatensatz
- uspto-grants-2010_04
- DOI