HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Hexynoic acid → 6-[3-(2-Hydroxy-1-methyl-ethylcarbamoyl)phenyl]-hex-5-ynoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Hexynoic acid | HCID 143036 | — |
| Edukt | N-(2-hydroxy-1-methyl-ethyl)-3-iodobenzamide | HCID 23730076 | — |
| Produkt | 6-[3-(2-Hydroxy-1-methyl-ethylcarbamoyl)phenyl]-hex-5-ynoic acid | HCID 11358215 | 99% |
Reaktionsschritte
The iodobenzamide (1)(2.00 g, 6.5 mmol) was coupled with 5-hexynoic acid using method B giving product (4)(1.87 g, 6.42 mmol; 99% yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07696382B2 |
| Quelldatensatz | uspto-grants-2010_04 |
| ORD ID | ord-4ef108aaf58548239c24a882e1ff897f |
| Quellennotiz | uspto-grants-2010_04 |