HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 64315Erstellt: 24. Oktober 2026
2-Bromo-1-(3-nitrophenyl)ethan-1-one → HCID 178513496, Verbindung
https://huagongshe.com/de/reaction/64315
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 2-Bromo-1-(3-nitrophenyl)ethan-1-one | HCID 75213 | — |
| Edukt | HCID 178513497 | HCID 178513497 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178513496 | HCID 178513496 | 11,4% |
Reaktionsschritte
A mixture of 5-amino-3-(4-phenoxyphenyl)-1H-pyrazole-4-carboxamide (29.4 mg, 0.1 mmol) and 2-bromo-1-(3-nitrophenyl)ethanone (24.4 mg, 0.1 mmol) in EtOH (2 mL) was stirred at 80° C. for 16 hr. The mixture was filtered to afford 5 mg of crude 2-(3-nitrophenyl)-6-(4-phenoxyphenyl)-1H-imidazo[1,2-b]pyrazole-7-carboxamide as a yellow solid. MS (ESI) m/e [M+1]+ 440.0.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US09447106B2 |
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| Quelldatensatz | uspto-grants-2016_09 |
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| ORD ID | ord-ee2d4ce594704a0985377a363f5590cf |
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| Quellennotiz | uspto-grants-2016_09 |
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