Ammonia → Carbamic acid, (aminothioxomethyl)-, ethyl ester
Reaktionsgleichung
[CH2:1]([O:3][C:4]([N:6]=[C:7]=[S:8])=[O:5])[CH3:2].[NH3:9]>C(O)C>[CH2:1]([O:3][C:4]([NH:6][C:7]([NH2:9])=[S:8])=[O:5])[CH3:2]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To 0.1 mole of ethoxycarbonyl isothiocyanate in ethanol (50 ml) is added 50 ml of a 2M ethanolic solution of ammonia. After 2 hours at room temperature, the precipitated product is collected by filtration and used in the next step.
Aufarbeitung
- filtrationthe precipitated product is collected by filtration
Quellen und Nachweise
- ORD-Eintrag
- ord-063d757386e8419c9033eb6b429a1fa3
- Quelldatensatz
- uspto-grants-2010_04
- Patentnummer
- USRE041289E1
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