HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Chlorophenol → 4-Chloro-1-(4-chlorophenoxy)-2-butanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Chlorophenol | HCID 4684 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 1,4-Dichloro-2-butanol | HCID 17021 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 4-Chloro-1-(4-chlorophenoxy)-2-butanol | HCID 13120349 | — |
Reaktionsschritte
4-Chloro-1-(4-chlorophenoxy)-2-butanol was prepared using the procedure of Preparation 7 from 45 g. (0.5 mole) of p-chlorophenol, 72 g. (0.5 mole) of 1,4-dichloro-2-butanol, 40 g. (1.0 mole) of sodium hydroxide and 400 ml. of water to give 85 g. (36.1%) of product which melted at 62°-64° C. after recrystallization from isopropanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04609735 |
| Quelldatensatz | uspto-grants-1986_09 |
| ORD ID | ord-b8932352aad64fcea11992d6264bd36e |
| Quellennotiz | uspto-grants-1986_09 |