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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 6475Erstellt: 23. Oktober 2026

Bis(2-chloroethyl) ether → 1,5-Bis(4-iodophenoxy)-3-oxapentane

https://huagongshe.com/de/reaction/6475

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBis(2-chloroethyl) etherHCID 8115—
Edukt4-IodophenolHCID 10894—
EduktSodium HydroxideHCID 14798—
Lösungsmittel1-ButanolHCID 263—
Produkt1,5-Bis(4-iodophenoxy)-3-oxapentaneHCID 19021957—

Reaktionsschritte

A mixture prepared by adding 3.08 g of sodium hydroxide and 40 ml of n-butanol to 15.4 g of 4-iodophenol was refluxed. 2 ml of n-butanol solution of 5.01 g of 1,5-dichloro-3-oxapentane was added dropwise to the above prepared mixture over a period of 5 minutes.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05248826
Quelldatensatzuspto-grants-1993_09
ORD IDord-de601d7504a04544afaf93084d42b5be
Quellennotizuspto-grants-1993_09