HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Bis(2-chloroethyl) ether → 1,5-Bis(4-iodophenoxy)-3-oxapentane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Bis(2-chloroethyl) ether | HCID 8115 | — |
| Edukt | 4-Iodophenol | HCID 10894 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Lösungsmittel | 1-Butanol | HCID 263 | — |
| Produkt | 1,5-Bis(4-iodophenoxy)-3-oxapentane | HCID 19021957 | — |
Reaktionsschritte
A mixture prepared by adding 3.08 g of sodium hydroxide and 40 ml of n-butanol to 15.4 g of 4-iodophenol was refluxed. 2 ml of n-butanol solution of 5.01 g of 1,5-dichloro-3-oxapentane was added dropwise to the above prepared mixture over a period of 5 minutes.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05248826 |
| Quelldatensatz | uspto-grants-1993_09 |
| ORD ID | ord-de601d7504a04544afaf93084d42b5be |
| Quellennotiz | uspto-grants-1993_09 |