Nitric Acid → Praseodymium trinitrate
Reaktionsgleichung
[O-2].[Pr+3:2].[O-2].[O-2].[Pr+3].[N+:6]([O-:9])([OH:8])=[O:7]>>[N+:6]([O-:9])([O-:8])=[O:7].[Pr+3:2].[N+:6]([O-:9])([O-:8])=[O:7].[N+:6]([O-:9])([O-:8])=[O:7]Komponenten
3
Reaktionsbedingungen
- Temperatur
- 100 °C
Versuchsvorschrift
Praseodymium oxide, Pr6O11 (1.55 g) was weighed into a silica crucible, concentrated nitric acid (2.5 ml) added and heated on a hot plate until the oxide had dissolved and the acid evaporated (~2 hr). The crucible and contents were heated overnight in an oven at 100° C. The praseodymium nitrate was dissolved in water, transferred to a volumetric flask (25 ml) and made up to volume.
Aufarbeitung
- additionadded
- dissolutionhad dissolved
- customthe acid evaporated (~2 hr)
- dissolutionThe praseodymium nitrate was dissolved in water
- customtransferred to a volumetric flask
Quellen und Nachweise
- ORD-Eintrag
- ord-96b7ab0f6e944620aea0074cb9db4942
- Quelldatensatz
- uspto-grants-1986_09
- Patentnummer
- US04610975
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