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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 64919Erstellt: 24. Oktober 2026

2-Methylpyridine → 2-(2,2-Dichlorovinyl)-benzyl 2-(4-chlorophenyl)-isovalerate

https://huagongshe.com/de/reaction/64919

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-MethylpyridineHCID 7975—
Edukt2-(4-Chlorophenyl)-3-methylbutanoyl chlorideHCID 4178001—
Edukt2-(2,2-Dichlorovinyl)-benzaldehydeHCID 13713131—
LösungsmittelTolueneHCID 1140—
Produkt2-(2,2-Dichlorovinyl)-benzyl 2-(4-chlorophenyl)-isovalerateHCID 13713135—

Reaktionsschritte

2.8 g (0.012 mole) of 2-(4-chlorophenyl)-isovaleryl chloride in 50 ml of absolute toluene are introduced into 1.2 g (0.013 mole) of -picoline and 3.2 g (0.015 mole) of 2-(2,2-dichlorovinyl)-benzaldehyde in a conical flask at room temperature, while stirring. After 30 minutes, the mixture is filtered under suction over silica gel, and washing is carried out with toluene.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04611010
Quelldatensatzuspto-grants-1986_09
ORD IDord-0f238b4ef3e5448f8833fd83cb856d4f
Quellennotizuspto-grants-1986_09