Dimethyloctylamine → HCID 178419187, Verbindung

HRID 649502

Reaktionsgleichung

Reaktionsgleichung von HRID 649502
[CH2:1]([N:9]([CH3:11])[CH3:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[BH3:12].C(N(CC)CC)C>C(N(CC)CC)C>[BH3:12].[CH2:1]([N:9]([CH3:11])[CH3:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Komponenten

4

Edukt 2

HCID 16224DimethyloctylamineHCID 264094borane;N,N-diethylethanamine

Produkt 1

HCID 178419187HCID 178419187, VerbindungAusbeute 89 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8471TriethylamineLösungsmittel

Versuchsvorschrift

Octyldimethylamine (20.4 grams; 0.130 mole) was heated with triethylamine borane (1.9 grams; 0.130 mole) at reflux temperature until 12.8 grams (98%) of triethylamine had been collected in a cold trap. The reaction residue was distilled at reduced pressure to give N-octyl-N,N-dimethylamine borane boiling at 98°-100° C./0.9 mm. Hg. (19.6 grams; 89% yield).

Aufarbeitung

  1. customhad been collected in a cold trap
  2. distillationThe reaction residue was distilled at reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-d602c547b2d447c5a70a59f83b9251c5
Quelldatensatz
uspto-grants-1988_04
Patentnummer
US04740504

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