HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Catechol → Guaiacol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Catechol | HCID 289 | — |
| Edukt | Methanol | HCID 887 | — |
| Produkt | Guaiacol | HCID 460 | — |
| Produkt | Phenol | HCID 996 | — |
Reaktionsschritte
When the temperature of the catalyst stratum reached 280° C., a starting compound mixture consisting of catechol and methyl alcohol in a molar mixing ratio of 1:3.44 was evaporated in a evaporator, and the resultant starting compound mixture gas was fed in a feeding rate of 10.5 g/min. together with a nitrogen gas into the reaction tube for 14 hours, to etherify catechol with methyl alcohol and to produce a dihydric phenol compound monoalkylether, i.e., guaiacol. The reaction mixture gas discharged from the reaction tube was cooled to a temperature of 40° C. The resultant liquefied product was collected from the reaction mixture.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05248835 |
| Quelldatensatz | uspto-grants-1993_09 |
| ORD ID | ord-bef22d2b530d42b096e5b7de282c4ca6 |
| Quellennotiz | uspto-grants-1993_09 |