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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 650462Erstellt: 24. Oktober 2026

Glycerol → Glyceryl Monooleate

https://huagongshe.com/de/reaction/650462

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktGlycerolHCID 753—
EduktOleic AcidHCID 445639—
LösungsmittelWaterHCID 962—
ProduktGlyceryl MonooleateHCID 5283468—

Reaktionsbedingungen

Temperatur50 °C

Reaktionsschritte

A mixture of oleic acid (1.5 g=5.32 mmoles), glycerol (0.57 g=6.2 mmoles), water (70 μl) and potato protein extract (100 mg) was stirred at 50° C. and a vacuum (<50 mbar) was applied to the system using an oil pump to remove water from the mixture. For comparison a similar reaction was run without vacuum in a stoppered tube. Samples were taken from the reaction mixtures periodically for analysis by GC. Progress curves for the reactions are given in FIG. 2. In the reaction cariied out under vacuum 4.43 mmoles of MG and 0.10 mmoles of DG were formed after 72 hours. 87% of the oleic acid was converted into acylglycerols. In the comparison reaction after 72 hours 3.51 mmoles of MG and 0.14 mmoles of DG were formed. The final conversion of oleic acid into acylglycerols was 71%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06274357B1
Quelldatensatzuspto-grants-2001_08
ORD IDord-eb93ae36da7340f1a833d29499ef6a99
Quellennotizuspto-grants-2001_08