HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,4-Dimethoxybenzoic acid → 5-Bromo-2,4-dimethoxybenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,4-Dimethoxybenzoic acid | HCID 7052 | — |
| Edukt | Bromine | HCID 24408 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 5-Bromo-2,4-dimethoxybenzoic acid | HCID 13505097 | 50% |
Reaktionsschritte
To a solution of 2,4-dimethoxybenzoic acid (4.0 g, 0.022 mol) in chloroform (60 ml) was added bromine (1.13 ml, 0.022 mol) in chloroform (20 ml) dropwise. After stiring overnight at room temperature the precipitate was filtered off and dried to afford the title compound as a white solid (2.87 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06277861B1 |
| Quelldatensatz | uspto-grants-2001_08 |
| ORD ID | ord-8aeaaf75fafb491db2f817b3286f1927 |
| Quellennotiz | uspto-grants-2001_08 |