HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → HCID 136332160, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Diethyl Ether | HCID 3283 | — |
| Edukt | 9-(1,3-Di-n-octanoyloxy-2-propoxymethyl)guanine | HCID 136332159 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 136332160 | HCID 136332160 | — |
Reaktionsschritte
A twofold stoichiometric excess of 3% hydrogen chloride in methanol is added to a solution of 1.0 g. of 9-(1,3-di-n-octanoyloxy-2-propoxymethyl)guanine in 20 ml methanol. Diethyl ether is added until precipitation is complete. The product is filtered, washed with ether, air dried and recrystallized to give 9-(1,3-di-n-octanoyloxy-2-propoxymethyl)guanine hydrochloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04612314 |
| Quelldatensatz | uspto-grants-1986_09 |
| ORD ID | ord-44085480c8624b88860ea735b0070417 |
| Quellennotiz | uspto-grants-1986_09 |