HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrazine hydrate (1:1) → HCID 178480237, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Edukt | 4-(2-Fluorobenzoyl)-1-methylpiperidine | HCID 13180317 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | HCID 178480237 | HCID 178480237 | 23,7% |
Reaktionsschritte
An autoclave was charged with 10.0 g of 4-(2-fluorobenzoyl)-1-methylpiperidine and 14 ml of hydrazine hydrate. The reaction was heated at 150° for 20 hrs, cooled, and poured into water. The resultant solid was collected. The solid was recrystallized twice from toluene to yield 2.4 g (23.7%) of product, mp 168°-170° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04670447 |
| Quelldatensatz | uspto-grants-1987_06 |
| ORD ID | ord-cdd33599bdaa477e8b872b2930c887a2 |
| Quellennotiz | uspto-grants-1987_06 |