HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Methylimidazole → HCID 178480862, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Methylimidazole | HCID 1390 | — |
| Edukt | 1-Chloro-4-(4-chlorobutyl)benzene | HCID 20082732 | — |
| Produkt | HCID 178480862 | HCID 178480862 | — |
Reaktionsschritte
Combine 6.1 g (0.03 mole) 1-chloro-4-(4-chlorobutyl)benzene with 2.5 g (0.03 mole) 1-methyl-1H-imidazole and heat at 120° C., following the course of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5). At the completion of the reaction, cool and triturate with ether, collect the solid and recrystallize from 50 ml hot acetone to obtain the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04613609 |
| Quelldatensatz | uspto-grants-1986_09 |
| ORD ID | ord-789f015a518643958156a7ed367e7d7e |
| Quellennotiz | uspto-grants-1986_09 |