1-Methylimidazole → HCID 178480862, Verbindung

HRID 65251

Reaktionsgleichung

Reaktionsgleichung von HRID 65251
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11]Cl)=[CH:4][CH:3]=1.[CH3:13][N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1>>[Cl-:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][N+:16]2[CH:17]=[CH:18][N:14]([CH3:13])[CH:15]=2)=[CH:4][CH:3]=1

Komponenten

3

Edukt 2

HCID 13901-MethylimidazoleHCID 200827321-Chloro-4-(4-chlorobutyl)benzene

Produkt 1

HCID 178480862HCID 178480862, Verbindung

Versuchsvorschrift

Combine 6.1 g (0.03 mole) 1-chloro-4-(4-chlorobutyl)benzene with 2.5 g (0.03 mole) 1-methyl-1H-imidazole and heat at 120° C., following the course of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5). At the completion of the reaction, cool and triturate with ether, collect the solid and recrystallize from 50 ml hot acetone to obtain the title compound.

Aufarbeitung

  1. customthe course of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5)
  2. customAt the completion of the reaction
  3. temperaturecool
  4. customtriturate with ether
  5. customcollect the solid
  6. customrecrystallize from 50 ml hot acetone

Quellen und Nachweise

ORD-Eintrag
ord-789f015a518643958156a7ed367e7d7e
Quelldatensatz
uspto-grants-1986_09
Patentnummer
US04613609

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