HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Hydroxybenzaldehyde → 5-(p-Methoxybenzylidene)-hydantoin
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Edukt | Glycine | HCID 750 | — |
| Edukt | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Edukt | Disodium glutamate | HCID 167560 | — |
| Produkt | 5-(p-Methoxybenzylidene)-hydantoin | HCID 94749 | — |
Reaktionsschritte
5-(p-Methoxybenzylidene)-hydantoin was prepared in the same manner as in Example 4, except that 46.8 g (0.25 mol) of sodium L-glutamate.monohydrate and 68.1 g (0.50 mol) of p-methoxybenzaldehyde were used in lieu of glycine and p-hydroxybenzaldehyde, respectively. During the reaction, the pH of the reaction mixture was 9.9 to 9.7.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04672127 |
| Quelldatensatz | uspto-grants-1987_06 |
| ORD ID | ord-21a593b0f39944088baeaee864758153 |
| Quellennotiz | uspto-grants-1987_06 |