HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → Acifluorfen sodium
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Acifluorfen | HCID 44073 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Acifluorfen sodium | HCID 44072 | 105,4% |
Reaktionsschritte
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04613360 |
| Quelldatensatz | uspto-grants-1986_09 |
| ORD ID | ord-9e9b4f013e6e41fe8d4ab299c0212c3e |
| Quellennotiz | uspto-grants-1986_09 |