Toluene → Dimethylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate

HRID 65332

Reaktionsgleichung

Reaktionsgleichung von HRID 65332
[Cl:1][C:2]1[CH:20]=[C:19]([C:21]([F:24])([F:23])[F:22])[CH:18]=[CH:17][C:3]=1[O:4][C:5]1[CH:6]=[CH:7][C:8]([N+:14]([O-:16])=[O:15])=[C:9]([CH:13]=1)[C:10]([OH:12])=[O:11].[C:25]1(C)C=CC=CC=1>>[Cl:1][C:2]1[CH:20]=[C:19]([C:21]([F:22])([F:23])[F:24])[CH:18]=[CH:17][C:3]=1[O:4][C:5]1[CH:6]=[CH:7][C:8]([N+:14]([O-:16])=[O:15])=[C:9]([CH:13]=1)[C:10]([O-:12])=[O:11].[CH3:25][NH2+:14][CH3:8]

Komponenten

3

Edukt 2

HCID 1140TolueneHCID 44073Acifluorfen

Produkt 1

HCID 21280075Dimethylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate

Versuchsvorschrift

5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (2.0 g) is dissolved in toluene and an excess of anhydrous dimethylamine is bubbled into the reaction mixture, the solvent removed in vacuo and the residue triturated with cold diethyl ether to give 1.1 g of product.

Aufarbeitung

  1. customan excess of anhydrous dimethylamine is bubbled into the reaction mixture
  2. customthe solvent removed in vacuo
  3. customthe residue triturated with cold diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-27c9993c0cab40a29c432342e69b7bed
Quelldatensatz
uspto-grants-1986_09
Patentnummer
US04613360

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