HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyltrimethylammonium methoxide → Benzyltrimethylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyltrimethylammonium methoxide | HCID 8504 | — |
| Edukt | Acifluorfen | HCID 44073 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Benzyltrimethylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate | HCID 14406043 | 20% |
Reaktionsschritte
A 20% aqueous methanolic solution of the salt is prepared by slurrying 5-(2-chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (22.2 g, 90% pure) in water (50 g) and adding a 40% solution of benzyltrimethylammonium methoxide (27 g) in methanol to pH 8. Additional water (0.8 g) is then added to give the desired concentration.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04613360 |
| Quelldatensatz | uspto-grants-1986_09 |
| ORD ID | ord-798f5eb68c4a4f6a8610f67340f5c705 |
| Quellennotiz | uspto-grants-1986_09 |