HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hexane → 4-Aza-4-cyclohexyl-2-(4-nitrophenyl)-1,6-heptadiene-3,5-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hexane | HCID 8058 | — |
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Edukt | Acrylamide, N-cyclohexyl- | HCID 137811 | — |
| Edukt | 2-(4-Nitrophenyl)prop-2-enoic acid | HCID 13278029 | — |
| Produkt | 4-Aza-4-cyclohexyl-2-(4-nitrophenyl)-1,6-heptadiene-3,5-dione | HCID 20027806 | — |
Reaktionsschritte
The title compound is prepared analogously to Example 1c starting from 40.5 g of α-(4-nitrophenyl)-acrylic acid, 26.7 g of oxalyl chloride and 26.8 g of N-cyclohexylacrylamide. Melting point 73°-74° (from hexane).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04677129 |
| Quelldatensatz | uspto-grants-1987_06 |
| ORD ID | ord-b7d2ac3db1a74de2b963d2e4700cea48 |
| Quellennotiz | uspto-grants-1987_06 |